Volume 66 Issue 8
Sep.  2022
Turn off MathJax
Article Contents
FU Chuan. Research on Calibration Method and Uncertainty Evaluation of Handheld Laser-Induced Breakdown Spectrometer[J]. Metrology Science and Technology, 2022, 66(8): 57-60. doi: 10.12338/j.issn.2096-9015.2022.0001
Citation: FU Chuan. Research on Calibration Method and Uncertainty Evaluation of Handheld Laser-Induced Breakdown Spectrometer[J]. Metrology Science and Technology, 2022, 66(8): 57-60. doi: 10.12338/j.issn.2096-9015.2022.0001

Research on Calibration Method and Uncertainty Evaluation of Handheld Laser-Induced Breakdown Spectrometer

doi: 10.12338/j.issn.2096-9015.2022.0001
  • Available Online: 2022-07-07
  • Publish Date: 2022-09-15
  • The development and application of handheld laser-induced breakdown spectrometers are introduced in this paper. Due to the lack of corresponding metrological technical specifications for this type of equipment, a metrological calibration method for handheld laser-induced breakdown spectrometers is proposed. The main metrological characteristics include detection limit, indication error, and repeatability. Based on the actual test data, the corresponding technical indicators are given. The uncertainty of indication error is analyzed in detail and the corresponding evaluation example is given. An effective evaluation method for the metrological traceability of handheld laser-induced breakdown spectrometer is given.
  • loading
  • [1]
    全国光电测量标准化技术委员会. 激光诱导击穿光谱法: GB/T 38257-2019[S]. 北京: 中国标准出版社, 2019.
    [2]
    Fu Y, Gu W, Hou Z, et al. Mechanism of signal uncertainty generation for laser-induced breakdown spectroscopy[J]. Frontiers of physics, 2020, 16(2): 22502.
    [3]
    王华东. 集成微区成像的LIBS系统实现及应用研究[D]. 合肥: 中国科学技术大学, 2019.
    [4]
    陈兴龙. 基于激光诱导击穿光谱的物质成份分析方法研究[D]. 合肥: 合肥工业大学, 2014.
    [5]
    王帅. 面向多形态物质元素分析的激光诱导击穿光谱快速检测技术研究[D]. 长春: 吉林大学, 2018.
    [6]
    李婧御, 陈宽, 陈国飞, 等. 手持式激光诱导击穿光谱仪对铝合金中镁钛元素的定量分析[J]. 激光与光电子学进展, 2019, 56(2): 237-243.
    [7]
    潘立剑, 陈蔚芳, 崔榕芳, 等. 基于激光诱导击穿光谱与径向基函数神经网络的铝合金定量分析[J]. 激光与光电子学进展, 2020, 57(19): 295-301.
    [8]
    王哲, 冯杰, 李政, 等. 提高激光诱导等离子光谱仪测量精度[J]. 清华大学学报(自然科学版), 2010, 50(8): 1263-1266. doi: 10.16511/j.cnki.qhdxxb.2010.08.010
    [9]
    赵辉, 黄辉, 李本涛, 等. 铝合金化学成分标准物质的研制[J]. 化学分析计量, 2016, 25(4): 8-10. doi: 10.3969/j.issn.1008-6145.2016.04.002
    [10]
    朱学纯, 尹晓辉, 韦志宏, 等. 含31个元素铝基光谱标准样品的制备及定值结果[J]. 铝加工, 2009(1): 4-9. doi: 10.3969/j.issn.1005-4898.2009.01.002
    [11]
    陈瑜, 刘功达, 吴洪军. 西南铝光谱标样的研制及其应用[C]. 中国有色金属学会第八届学术年会论文集. 长沙: 中南大学出版社, 2010: 465-471.
    [12]
    李成利, 朱学纯. 提高铝及铝合金光谱标准样品均匀性的探讨[J]. 铝加工, 2003(1): 29-33. doi: 10.3969/j.issn.1005-4898.2003.01.012
    [13]
    罗杨, 黎潮. 直读光谱仪测定铝合金中元素含量质量控制方法[J]. 化工管理, 2016(35): 179. doi: 10.3969/j.issn.1008-4800.2016.35.153
    [14]
    王蕾, 高峰, 孟涛, 等. 新型大气采样器校准方法研究及不确定度评定[J]. 计量科学与技术, 2021, 65(8): 46-50. doi: 10.12338/j.issn.2096-9015.2020.9005
    [15]
    Wang Z, Afgan M S, Gu W, et al. Recent advances in laser-induced breakdown spectroscopy quantification: From fundamental understanding to data processing[J]. Trends in analytical chemistry, 2021, 143: 116385. doi: 10.1016/j.trac.2021.116385
    [16]
    董贺伟, 郭瑞民, 崔文超, 等. 光梳光谱仪技术及其应用[J]. 计量技术, 2019(8): 6-9.
    [17]
    方立德, 徐潇潇, 赵计勋, 等. 恒流源对近红外光谱传感器测量不确定度的影响[J]. 计量学报, 2022, 43(3): 370-377. doi: 10.3969/j.issn.1000-1158.2022.03.11
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(1)  / Tables(6)

    Article Metrics

    Article views (777) PDF downloads(82) Cited by()
    Proportional views
    Related

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return