Development of Reference Materials for Sulfur Element Content in Isooctane

REN Danhua; ZHANG Airui; WANG Meiling; WANG Xiangnan; WANG Hai

doi:10.12338/j.issn.2096-9015.2022.0200

Volume 66 Issue 12

Feb. 2023

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REN Danhua, ZHANG Airui, WANG Meiling, WANG Xiangnan, WANG Hai. Development of Reference Materials for Sulfur Element Content in Isooctane[J]. Metrology Science and Technology, 2022, 66(12): 16-20. doi: 10.12338/j.issn.2096-9015.2022.0200

Citation:

REN Danhua, ZHANG Airui, WANG Meiling, WANG Xiangnan, WANG Hai. Development of Reference Materials for Sulfur Element Content in Isooctane[J]. Metrology Science and Technology, 2022, 66(12): 16-20. doi: 10.12338/j.issn.2096-9015.2022.0200

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Development of Reference Materials for Sulfur Element Content in Isooctane

doi: 10.12338/j.issn.2096-9015.2022.0200

1.
National Institute of Metrology, Beijing 100029, China
2.
Beijing University of Chemical Technology, Beijing 100029, China

Received Date: 2022-08-11
Accepted Date: 2022-08-22

Available Online: 2022-11-08

Publish Date: 2022-12-18

Abstract

Abstract

Certified reference materials (CRM) for sulfur content in light oil-GBW(E)110117, which can be used for the calibration of the UV fluorescence sulfur meter and X-ray fluorescence sulfur meter, was developed to solve the problems in the preparation and characterization of the CRM. The CRM is based on isooctane and polysulfide compounds, and was certified by the internationally recognized primary method of isotope dilution inductively coupled plasma mass spectrometry (ID ICP-MS), and the homogeneity and stability of the CRM candidates were evaluated by UV fluorescence. The results showed that the certified value and its expanded uncertainty were 10.58 mg/kg and 4.3% (k=2), respectively.
- light oil,
- sulfur,
- isooctane,
- certified reference materials,
- ID ICP-MS,
- uncertainty

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References(32)

References

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