Development of Certified Reference Material for Forchlorfenuron Residue in Cucumber Powder

YANG Mengrui; SHI Haochuan; XU Qi; CHEN Wenwen; ZHANG Liyuan; ZHOU Jian; WANG Min

doi:10.12338/j.issn.2096-9015.2023.0318

Volume 67 Issue 10

Oct. 2023

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Article Navigation > Metrology Science and Technology > 2023 > 67(10): 30-36

YANG Mengrui, SHI Haochuan, XU Qi, CHEN Wenwen, ZHANG Liyuan, ZHOU Jian, WANG Min. Development of Certified Reference Material for Forchlorfenuron Residue in Cucumber Powder[J]. Metrology Science and Technology, 2023, 67(10): 30-36. doi: 10.12338/j.issn.2096-9015.2023.0318

Citation:

YANG Mengrui, SHI Haochuan, XU Qi, CHEN Wenwen, ZHANG Liyuan, ZHOU Jian, WANG Min. Development of Certified Reference Material for Forchlorfenuron Residue in Cucumber Powder[J]. Metrology Science and Technology, 2023, 67(10): 30-36. doi: 10.12338/j.issn.2096-9015.2023.0318

Citation:

YANG Mengrui, SHI Haochuan, XU Qi, CHEN Wenwen, ZHANG Liyuan, ZHOU Jian, WANG Min. Development of Certified Reference Material for Forchlorfenuron Residue in Cucumber Powder[J]. Metrology Science and Technology, 2023, 67(10): 30-36. doi: 10.12338/j.issn.2096-9015.2023.0318

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Development of Certified Reference Material for Forchlorfenuron Residue in Cucumber Powder

doi: 10.12338/j.issn.2096-9015.2023.0318

Institute of Quality Standard and Testing Technology for Agro-Products, Chinese Academy of Agricultural Sciences, Beijing 100081, China

Received Date: 2023-11-28
Accepted Date: 2023-12-05
Rev Recd Date: 2023-12-06

Available Online: 2023-12-13

Publish Date: 2023-10-18

Abstract

Abstract

Matrix certified reference materials (CRMs) play a crucial role in validating analytical methods and ensuring quality control. To enhance the accuracy and reliability of risk assessments for plant growth regulators, we have developed a certified reference material (CRM) for forchlorfenuron in cucumber powder, thereby improving the measurement quality of forchlorfenuron residues in cucumbers. The CRM was prepared through processes including pulping, drug-adding, homogenization, freeze-drying, grinding, sieving, mixing, and encapsulation. The liquid chromatography-tandem isotope dilution mass spectrometry (ID-LC/MS/MS) method was optimized and established for the quantification of the CRM. The certified value of forchlorfenuron in cucumber powder was determined to be 14.7 mg/kg with an expanded uncertainty of 2.7 mg/kg (k=2). Furthermore, the homogeneity of the material was assessed, along with its long-term stability at −20°C over nine months and short-term stability at 40°C over nine days. The study comprehensively evaluated uncertainties introduced by characterization, homogeneity, and stability assessments.
- metrology,
- cucumber matrix certified reference material,
- forchlorfenuron,
- quantification,
- homogeneity,
- stability

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References(30)

References

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