Development of Reference Material for Calcium and Phosphorus in Chicken Formula Feed

YAN Hua; XU Siyuan; HU Shen; ZHANG Zhenhao; JIA Zheng; FAN Xia

doi:10.12338/j.issn.2096-9015.2023.0324

Volume 67 Issue 10

Oct. 2023

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Article Navigation > Metrology Science and Technology > 2023 > 67(10): 62-69

YAN Hua, XU Siyuan, HU Shen, ZHANG Zhenhao, JIA Zheng, FAN Xia. Development of Reference Material for Calcium and Phosphorus in Chicken Formula Feed[J]. Metrology Science and Technology, 2023, 67(10): 62-69. doi: 10.12338/j.issn.2096-9015.2023.0324

Citation:

YAN Hua, XU Siyuan, HU Shen, ZHANG Zhenhao, JIA Zheng, FAN Xia. Development of Reference Material for Calcium and Phosphorus in Chicken Formula Feed[J]. Metrology Science and Technology, 2023, 67(10): 62-69. doi: 10.12338/j.issn.2096-9015.2023.0324

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Development of Reference Material for Calcium and Phosphorus in Chicken Formula Feed

doi: 10.12338/j.issn.2096-9015.2023.0324

1.
Institute of Quality Standard and Testing Technology for Agro-Products, Chinese Academy of Agricultural Sciences, Beijing 100081, China
2.
Hubei Province Institute of Veterinary Drug, Wuhan 430070, China

Received Date: 2023-11-30
Accepted Date: 2023-12-04
Rev Recd Date: 2023-12-11

Available Online: 2023-12-15

Publish Date: 2023-10-18

Abstract

Abstract

To address the needs of food safety monitoring, a certified reference material (CRM) for calcium and phosphorus in chicken formula feed was developed. The CRM underwent sample pretreatment using microwave digestion, followed by quantification of calcium and phosphorus content using an inductively coupled plasma optical emission spectrometer (ICP-OES). The homogeneity and stability of the CRM were systematically analyzed, and uncertainties were evaluated. The results demonstrate that the CRM exhibits excellent homogeneity and stability, with certified values of 1.221% for calcium and 0.687% for phosphorus, and expanded uncertainties of 0.117% and 0.091% (k=2), respectively. The CRM can be stored for 16 months at −18 ℃. This development fulfills the requirements for feed quality and safety monitoring and provides essential technical support for calibration, quality control, and method validation in the analysis of calcium and phosphorus in formulated feed samples.
- metrology,
- chicken formula feed,
- calcium,
- phosphorous,
- reference material,
- characterization,
- uncertainty

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References(33)

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