立式铜固定点炉量值溯源方法研究

    Research on the Traceability Method of Quantity Value for Vertical Copper Fixed Point Furnace

    • 摘要: 国内在校准标准铂铑10-铂热电偶标准组时,使用的立式铜固定点炉的温度多采用ITS-90名义值,没有现行有效的校准方法可溯源至高温基准。针对这一问题,设计了一套校准方案和装置,利用可旋转支架,可实现光电高温计交替垂直测量立式铜固定点炉和水平测量基准铜固定点黑体的比较方法。该方法解决了立式铜固定点炉量值无法溯源的问题,保证了立式铜固定点炉与高温基准温标的一致性。以某台热电偶校准用立式铜固定点炉为例,介绍了校准实验装置、校准方法以及壁温、发射率修正,经比较并修正后,得到校准的温度值,并对不确定度进行评估。实验结果表明,某热电偶校准用立式铜固定点炉的校准温度值为1084.61℃,不确定度为0.09℃(k=2)。该方法的实现不仅解决了立式铜固定点炉的量值溯源问题,同时也为银点以下中低温固定点黑体向接触测温基准量值溯源提供一种新的思路。

       

      Abstract: In the calibration of standard platinum - rhodium 10 - platinum thermocouple standard groups in China, a problem occurs: the vertical copper fixed - point furnace uses the ITS - 90 nominal value but lacks traceability to the high - temperature primary standard, which may cause inaccurate calibration results. This paper devises a calibration scheme with a rotatable - bracket - based device. A photoelectric pyrometer can measure the vertical copper fixed - point furnace vertically and the reference copper fixed - point blackbody horizontally. This comparative method resolves the non - traceability issue and ensures compliance with the high - temperature reference scale. Taking a thermocouple - calibration vertical copper fixed - point furnace as an example, the paper details the calibration device, method, and wall - temperature and emissivity corrections. After comparison and correction, the calibrated temperature is 1084.61 °C, with an uncertainty of 0.09 °C (k = 2). The method resolves the vertical copper fixed - point furnace's traceability problem and offers a new way for the traceability of medium - and low - temperature fixed - point blackbodies below the silver point to the contact temperature primary standard, enabling more accurate calibrations in related fields.

       

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