Volume 65 Issue 6
Jul.  2021
Turn off MathJax
Article Contents
LI Xianjiang, GUO Zhen, ZHAO Guangliang, LI Xiuqin, ZHANG Qinghe, LI Hongmei. Development of Certified Reference Materials of Patulin in Acetonitrile GBW(E)100674[J]. Metrology Science and Technology, 2021, 65(6): 34-38, 24. doi: 10.12338/j.issn.2096-9015.2020.9047
Citation: LI Xianjiang, GUO Zhen, ZHAO Guangliang, LI Xiuqin, ZHANG Qinghe, LI Hongmei. Development of Certified Reference Materials of Patulin in Acetonitrile GBW(E)100674[J]. Metrology Science and Technology, 2021, 65(6): 34-38, 24. doi: 10.12338/j.issn.2096-9015.2020.9047

Development of Certified Reference Materials of Patulin in Acetonitrile GBW(E)100674

doi: 10.12338/j.issn.2096-9015.2020.9047
  • Available Online: 2021-06-09
  • Publish Date: 2021-07-08
  • A solution Certified Reference Material (CRM) of patulin was developed and has been officially approved with the code of GBW(E)100674. This CRM was prepared by using the gravimetric-volumetric method with solid materials of the patulin purity CRM GBW(E)100673. According to the general and statistical principles for characterization of reference materials in JJF 1343-2012, homogeneity and stability tests were carried out with liquid chromatography. Uncertainty was evaluated in consideration of solid purity, solution preparation, homogeneity, short-term stability, and long-term stability. The certified value of the patulin solution is 100 µg/mL with an expanded uncertainty of 2% (k=2). The atulin solution CRM with a traceable and accurate value can support food safety tests in China.
  • loading
  • [1]
    Wright S A I. Patulin in food[J]. Curr. Opin. Food Sci, 2015, 5: 105-109. doi: 10.1016/j.cofs.2015.10.003
    [2]
    Moake M M, Padilla-Zakour O I, Worobo R W. Comprehensive Review of Patulin Control Methods in Foods[J]. Compr. Rev. Food Sci. F, 2005, 4(1): 8-21. doi: 10.1111/j.1541-4337.2005.tb00068.x
    [3]
    Li X, Li H, Li X, et al. Determination of trace patulin in apple-based food matrices[J]. Food Chem, 2017, 233: 290-301. doi: 10.1016/j.foodchem.2017.04.117
    [4]
    Rychlik M, Kircher F, Schusdziarra V, et al. Absorption of the mycotoxin patulin from the rat stomach[J]. Food Chem. Toxicol, 2004, 42(5): 729-735. doi: 10.1016/j.fct.2003.12.015
    [5]
    Schumacher D M, Müller C, Metzler M, et al. DNA-DNA cross-links contribute to the mutagenic potential of the mycotoxin patulin[J]. Toxicol. Lett, 2006, 166(3): 268-75. doi: 10.1016/j.toxlet.2006.08.002
    [6]
    Sadok I, Stachniuk A, Staniszewska M. Developments in the Monitoring of Patulin in Fruits Using Liquid Chromatography: an Overview[J]. Food Anal. Methods, 2019, 12(1): 76-93. doi: 10.1007/s12161-018-1340-9
    [7]
    Li X, Li H, Ma W, et al. Determination of patulin in apple juice by single-drop liquid-liquid-liquid microextraction coupled with liquid chromatography-mass spectrometry[J]. Food Chem, 2018, 257: 1-6. doi: 10.1016/j.foodchem.2018.02.077
    [8]
    Li X, Ma W, Zhang Q. Determination of patulin in apple juice by amine-functionalized solid-phase extraction coupled with isotope dilution liquid chromatography tandem mass spectrometry[J]. J. Sci. Food Agric, 2020, 101(5): 1767-1771. doi: 10.1002/jsfa.10790
    [9]
    Zhao M, Shao H, Ma J, et al. Preparation of core-shell magnetic molecularly imprinted polymers for extraction of patulin from juice samples[J]. J. Chromatogr. A, 2020, 1615: 460751. doi: 10.1016/j.chroma.2019.460751
    [10]
    Ouhibi S, Vidal A, Martins C, et al. LC-MS/MS methodology for simultaneous determination of patulin and citrinin in urine and plasma applied to a pilot study in colorectal cancer patients[J]. Food Chem. Toxicol, 2020, 136: 110994. doi: 10.1016/j.fct.2019.110994
    [11]
    Zhao M, Shao H, Ma J, et al. The determination of patulin from food samples by using dual-dummy molecularly imprinted solid-phase extraction coupled with HPLC-MS/MS[J]. J. Chromatogr. B, 2019, 1125: 121714. doi: 10.1016/j.jchromb.2019.121714
    [12]
    Sadok I, Szmagara A, Staniszewska M M. The validated and sensitive HPLC-DAD method for determination of patulin in strawberries[J]. Food Chem, 2018, 245: 364-370. doi: 10.1016/j.foodchem.2017.10.093
    [13]
    Yu Y, Fan Z. Determination of patulin in apple juice using magnetic solid-phase extraction coupled with high-performance liquid chromatography[J]. Food Addit. Contam. A, 2017, 34(2): 273-281.
    [14]
    Wang Y, Wen Y, Ling Y.-C. Graphene Oxide-Based Magnetic Solid Phase Extraction Combined with High Performance Liquid Chromatography for Determination of Patulin in Apple Juice[J]. Food Anal. Methods, 2017, 10(1): 210-218. doi: 10.1007/s12161-016-0570-y
    [15]
    韦琪, 苏福海. 甲卡西酮纯度标准物质的研制[J]. 计量科学与技术, 2020(11): 10-16.
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(5)

    Article Metrics

    Article views (272) PDF downloads(34) Cited by()
    Proportional views
    Related

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return