Volume 66 Issue 10
Sep.  2022
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REN Danhua, ZHANG Airui, WANG Meiling, WANG Xiangnan, WANG Hai. Development of Reference Materials for Phosphorus Element in Light Oil Products[J]. Metrology Science and Technology, 2022, 66(10): 41-45, 9. DOI: 10.12338/j.issn.2096-9015.2022.0161
Citation: REN Danhua, ZHANG Airui, WANG Meiling, WANG Xiangnan, WANG Hai. Development of Reference Materials for Phosphorus Element in Light Oil Products[J]. Metrology Science and Technology, 2022, 66(10): 41-45, 9. DOI: 10.12338/j.issn.2096-9015.2022.0161
shu

Development of Reference Materials for Phosphorus Element in Light Oil Products

  • 1.

    National Institute of Metrology, Beijing 100029, China

  • 2.

    Beijing University of Chemical Technology, Beijing 100029, China

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  • Received Date: July 05, 2022
  • Accepted Date: July 12, 2022
  • Available Online: September 08, 2022
    Graphical Abstract
    • Abstract
  • In this paper, a certified reference material (CRM) for phosphorus in isooctane (GBW11211) was developed to meet the national standard for measuring the content of phosphorus in light oil. The CRM was prepared with isooctane and phosphorus element standard hydrocarbon oil as raw materials, and inductively coupled plasma mass spectrometry (ICP-MS) and inductively coupled plasma optical emission spectrometry (ICP-OES) were used as the characterization methods for the CRM, which were jointly characterized by several laboratories, and the homogeneity and stability of the CRM for elemental phosphorus in isooctane were evaluated. The results show that the certified value of the CRM of the phosphorus component in isooctane is 0.44 mg·kg−1, with an extended uncertainty of 0.05 mg·kg−1 (k =2), and the validity period is 36 months. The CRM can be used for quality control and method verification of related oil products.
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    • References (21)
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